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The continuous reactor is used in the leaching operation.An autoclave is the most suitable reactor for leaching at high pressure and temperature.The condenser temporarily allows gaseous emission to escape from the reactor hence prevents any pressure build-up.One should calculate the leaching extent according to the final volume of leach liquor, or one can add DI water to make up to the initial volume and then analyses the sample.PTFE/Teflon and metallic reactors are suitable for leaching at higher temperatures as they can withstand high pressure.An autoclave is a metallic reactor where heating is done by coils and stirring is done mechanically.To withstand higher pressure condenser is generally fitted with glass reactors.
The continuous reactor is used in the leaching operation. Leaching at high temperatures generates water vapor. Often there are gaseous emissions during leaching. These gaseous emissions, along with water vapor, increase the pressure inside a closed reactor. Glass being a brittle material, breaks above a certain pressure. To withstand higher pressure condenser is generally fitted with glass reactors. The condenser temporarily allows gaseous emission to escape from the reactor hence prevents any pressure build-up. Later the emissions are condensed to liquid droplets, which fall back to the reactor. Condensers are not always 100% efficient. Some gaseous emissions escape through condensers, and one can often witness the loss in the volume of leach liquor. One should calculate the leaching extent according to the final volume of leach liquor, or one can add DI water to make up to the initial volume and then analyses the sample. PTFE/Teflon and metallic reactors are suitable for leaching at higher temperatures as they can withstand high pressure. Since they can withstand high-pressure condenser is not required. The pressure inside a reactor directly depends on the leaching temperature. Pressure can be varied independently only in an autoclave. An autoclave is a metallic reactor where heating is done by coils and stirring is done mechanically. Additional fitting is provided in the reactor to increase pressure and temperature independently. An autoclave is the most suitable reactor for leaching at high pressure and temperature.
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